Dual-Catalyst Acceleration of Tandem Disulfide Cleavage and Baylis–Hillman Synthesis of 2 H-1-Benzothiopyran Derivatives

Nyoni, Dubekile; Lobb, Kevin A; Kaye, Perry T

Title: Dual-Catalyst Acceleration of Tandem Disulfide Cleavage and Baylis–Hillman Synthesis of 2 H-1-Benzothiopyran Derivatives
Creator: Nyoni, Dubekile
Creator: Lobb, Kevin A
Creator: Kaye, Perry T
Subject: To be catalogued
Date Issued: 2013
Date: 2013
Type: text
Type: article
Identifier: http://hdl.handle.net/10962/448898
Identifier: vital:74769
Identifier: xlink:href="https://doi.org/10.1080/00397911.2012.673449"
Description: While both 1,8-diazabicyclo[5.4.0]undec-7-ene and triphenylphosphine catalyze tandem Baylis–Hillman reaction/disulfide cleavage of 2,2′-dithiodibenzaldehyde independently, when used together as a dual-catalyst system, the overall yields of the cyclized 2H-1-benzothiopyrans are consistently greater and the reaction time decreases dramatically.
Format: computer
Format: online resource
Format: application/pdf
Format: 1 online resource (5 pages)
Format: pdf
Publisher: Taylor and Francis
Language: English
Relation: Synthetic Communications
Relation: Nyoni, D., Lobb, K.A. and Kaye, P.T., 2013. Dual-Catalyst Acceleration of Tandem Disulfide Cleavage and Baylis–Hillman Synthesis of 2 H-1-Benzothiopyran Derivatives. Synthetic Communications, 43(13), pp.1837-1841
Relation: Synthetic Communications volume 43 number 13 p. 1837 2013 1532-2432
Rights: Publisher
Rights: Use of this resource is governed by the terms and conditions of the Taylor and Francis Online Terms and Conditions Statement (https://www.tandfonline.com/terms-and-conditions)
Rights: Closed Access

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Kaye, Perry T (Distinguished Fellow Emeritus Professor)

Lobb, Kevin Allan (Assoc Prof)

RU Department of Chemistry

SDG 03. Good Health and Well-Being

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